Subject: Methods of instrumental analysis in environmental protection (17.Z570A )
Native organizations units: No data
Study programmes of the course:
| Type of studies | Title |
|---|---|
| Master Academic Studies | Environmental engineering (Godina: 1, Summer) |
Educational goal:
- To provide knowledge to environmental engineering students on instrumental methods for pollutants analysis in the air and water: AAS, UV/VIS, HPLC/DAD, GC/MS - To provide students knowledge on the principles of sample preparation techniques - To develop students skills for sample preparation and appropriate instrumental method usage - To develop knowledge and skills in statistical processing of analytical data - To provide students knowledge on the quality control of pollutant analysis
Educational outcome:
Students should be able to: - Select and implement the appropriate instrumental method of pollutants analysis in the air and water - Select and use the appropriate sample preparation technique - Evaluate analytical results by one of the statistical softwares (eg Excel), - Make written report on the analytical results - Implement the quality control of the obtained analytical results
Course content:
Methodology in instrumental analysis and quality control. Organization and functioning of the reference and accredited laboratories. Methods of air and water sampling and extraction of inorganic and organic pollutants. Determination of inorganic pollutants in the air and water by atomic absorption spectroscopy (AAS) and ultraviolet - visible spectroscopy (UV/VIS). Gravimetric methods for the determination of suspended particulate matter (PM) in the air. Identification of organic pollutants by gas chromatography (GC) and liquid chromatography (HPLC) with different detectors and a combined method of gas chromatography and mass spectrometry (GC/MS). Interpretation and statistical analysis of measurement results and comparing the results with national and European regulations in environmental protection. The subject consists of experimental laboratory exercises that follow the theoretical fundamentals. Student independently presents the results of the exercises in the form of a report. Laboratory exercises: Determination of metal cations in water samples by atomic absorption spectrometry. Determination of ozone, ammonia, nitrogen and sulfur oxides in air samples using ultraviolet - visible spectroscopy. Determination of ammonia, nitrate, nitrite and phosphorus concentrations in water samples using ultraviolet - visible spectroscopy. Identification of organic pollutants by GC-MS. Identification of organic pollutants by liquid chromatography (HPLC-DAD) by remote work in the Laboratory via the web: WARIAL. Statistical analysis of the results and writing laboratory reports.
Teaching methods:
Lectures, interactive sessions, consultations and experimental laboratory exercises. During the semester, students are required to attend lectures and exercises, and to present experimental results of laboratory exercises in the form of reports. After successfully completed pre-exam requirements, students take to the final exam consisting of two parts: written and oral. The written exam can be taken in the form of two tests.
Literature:
| Authors | Title | Year | Publisher | Language |
|---|---|---|---|---|
| 2010 | English | |||
| I. Mihajlović | Elеktrоnski nаstаvni mаtеriјаli rаzviјеni u оkviru |
2019 | Serbian language | |
| Ј. Мišоvić, Т. Аst | Instrumеntаlnе mеtоdе hеmiјskе аnаlizе | 1994 | TMF Bеоgrаd | Serbian language |
| 2007 | English | |||
| 2007 | English | |||
| М. Тоdоrоvić, P. Đurđеvić, V. Аntоniјеvić | Оptičkе mеtоdе instrumеntаlnе аnаlizе | 1997 | Hеmiјski fаkultеt, Bеоgrаd | Serbian language |
| S. Milosavljevic | Strukturne instrumentalne metode | 1996 | Hemijski fakultet, Beograd | Serbian language |
Knowledge evaluation:
| Course activity | Pre-examination | Obligations | Number of points |
|---|---|---|---|
| Written part of the exam - tasks and theory | No | Yes | 40.00 |
| Lecture attendance | Yes | Yes | 5.00 |
| Laboratory exercise defence | Yes | Yes | 20.00 |
| Laboratory exercise attendance | Yes | Yes | 5.00 |
| Oral part of the exam | No | Yes | 30.00 |
Lecturers:
Istraživač saradnik Dmitrašinović Sonja
Research Associate
Laboratory classes
vanr. prof. dr Mihajlović Ivana
Associate Professor
Lectures
Asistent - dr nauka dr Novaković Mladenka
Assistant with PhD
Laboratory classes
vanr. prof. dr Petrović Maja
Associate Professor
Lectures
Naučni saradnik Obrovski Boris
Science Associate
Laboratory classes
Faculty of Technical Sciences
© 2024. Faculty of Technical Sciences.
Contact:
Address: Trg Dositeja Obradovića 6, 21102 Novi Sad
© 2024. Faculty of Technical Sciences.